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SYNTHESIS OF MONO-, DI-, AND POLYNITROXIDES. CLASSIFICATION OF ESRSPECTRA OF FLEXIBLE DINITROXIDES DISSOLVED IN LIQUIDS AND GLASSES [electronic resource].

Published:
Washington, D.C. : U.S. Atomic Energy Commission, 1969.
Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy.
Physical Description:
48 pages : digital, PDF file
Additional Creators:
U.S. Atomic Energy Commission and United States. Department of Energy. Office of Scientific and Technical Information
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Summary:
The synthesis of flexible biradical strain-gauges which could be anchored onto two sites of a deformable biological structure had been attempted. Qualitative relationships between the possible conformations of the biradicals and the observed ESR spectra provide guidelines for further synthetic work. Some of the nitroxides synthesized and characterized are: R-CO-R₁-N-(CH₂){sub n}-R₂-N-CO-R, where R is 1-oxyl-2,2,6,6-tetramethyl pyrroline bonded at the 3-position, n = 2,3 and R{sub 1,2} = -H; -C₁₈₃₇; -CH₂COOH; -CH₂COOC₂H₅; -CH₂CONH(CH₂)₂N(CH₃)₂; -CH₂CONH(CH₂)₂N⁺(CH₃) -CH₂CO-imidazolide.
Report Numbers:
E 1.99:ucrl--19419
ucrl--19419
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Note:
Published through SciTech Connect.
11/01/1969.
"ucrl--19419"
Journal of the American Chemical Society 0 0 ISSN 0002-7863; JACSAT FT
Calvin, M.; Gill, D.; Klein, M.P.; Wang, H.H.; Entine, G.; Ferruti, P.
Ernest Orlando Lawrence Berkeley NationalLaboratory, Berkeley, CA (US)
Funding Information:
DE-AC02-05CH11231
View MARC record | catkey: 14395843