Actions for Determination of dibutylbutylphosphonate in the presence of tributylphosphate by gas liquid chromatography [electronic resource].

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Determination of dibutylbutylphosphonate in the presence of tributylphosphate by gas liquid chromatography [electronic resource].

Published
Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy, 1976.
Physical Description
Pages: 25 : digital, PDF file
Additional Creators
United States. Department of Energy. Office of Scientific and Technical Information
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Summary
A gas chromatographic determination of dibutylbutyl-phosphonate in the presence of tributylphosphate was developed. The separation was done on a 183 cm by 3 mm stainless steel column packed with 10 percent Carbowax 20M--TPA on 80/100 mesh Chromosorb W AW and detected by flame ionization. A nitrogen carrier gas flow of 40 cm/sup 3//min and an oven temperature of 180/sup 0/C produced optimum resolution and column efficiency. The use of temperature programming reduced retention times and thus analysis time. An internal standard of 10 percent v/v n-tridecane was added to all samples and standards.
Report Numbers
E 1.99:arh-sa-249
E 1.99: conf-760668-1
conf-760668-1
arh-sa-249
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Note
Published through SciTech Connect.
05/01/1976.
"arh-sa-249"
" conf-760668-1"
31. annual northwest regional American Chemical Society meeting, Reno, NV, USA, 14 Jun 1976.
Johnson, S.J.
Atlantic Richfield Hanford Co., Richland, Wash. (USA)
Funding Information
E(45-1)-2130
View MARC record | catkey: 14397946