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Tank 103, 219-S Facility at 222-S Laboratory, analytical results for the final report [electronic resource].

Published:
Washington, D.C. : United States. Dept. of Energy, 1998.
Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy.
Physical Description:
128 pages : digital, PDF file
Additional Creators:
United States. Department of Energy and United States. Department of Energy. Office of Scientific and Technical Information
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Summary:
This is the final report for the polychlorinated biphenyls analysis of Tank-103 (TK-103) in the 219-S Facility at 222-S Laboratory. Twenty 1-liter bottles (Sample numbers S98SO00074 through S98SO00093) were received from TK-103 during two sampling events, on May 5 and May 7, 1998. The samples were centrifuged to separate the solids and liquids. The centrifuged sludge was analyzed for PCBs as Aroclor mixtures. The results are discussed on page 6. The sample breakdown diagram (Page 114) provides a cross-reference of sample identification of the bulk samples to the laboratory identification number for the solids. The request for sample analysis (RSA) form is provided as Page 117. The raw data is presented on Page 43. Sample Description, Handling, and Preparation Twenty samples were received in the laboratory in 1-Liter bottles. The first 8 samples were received on May 5, 1998. There were insufficient solids to perform the requested PCB analysis and 12 additional samples were collected and received on May 7, 1998. Breakdown and sub sampling was performed on May 8, 1998. Sample number S98SO00084 was lost due to a broken bottle. Nineteen samples were centrifuged and the solids were collected in 8 centrifuge cones. After the last sample was processed, the solids were consolidated into 2 centrifuge cones. The first cone contained 9.7 grams of solid and 13.0 grams was collected in the second cone. The wet sludge from the first centrifuge cone was submitted to the laboratory for PCB analysis (sample number S98SO00102). The other sample portion (S98SO00103) was retained for possible additional analyses.
Report Numbers:
E 1.99:hnf-sd-wm-dp--306
hnf-sd-wm-dp--306
Subject(s):
Other Subject(s):
Note:
Published through SciTech Connect.
06/18/1998.
"hnf-sd-wm-dp--306"
"DE99050724"
"EW3120074"
Fuller, R.K.
Fluor Daniel Hanford Inc., Richland, WA (United States)
Type of Report and Period Covered Note:
Topical; 06/01/1998 - 06/01/1998
Funding Information:
AC06-96RL13200
View MARC record | catkey: 14413503