The effect of sample preparation methods on glass performance [electronic resource].
- Published
- Washington, D.C : United States. Dept. of Energy. Office of the Assistant Secretary for Defense Programs, 1990.
Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy. - Physical Description
- Pages: (23 pages) : digital, PDF file
- Additional Creators
- Lawrence Livermore National Laboratory, United States. Department of Energy. Office of the Assistant Secretary for Defense Programs, and United States. Department of Energy. Office of Scientific and Technical Information
Access Online
- Restrictions on Access
- Free-to-read Unrestricted online access
- Summary
- A series of experiments was conducted using SRL 165 synthetic waste glass to investigate the effects of surface preparation and leaching solution composition on the alteration of the glass. Samples of glass with as-cast surfaces produced smooth reaction layers and some evidence for precipitation of secondary phases from solution. Secondary phases were more abundant in samples reacted in deionized water than for those reacted in a silicate solution. Samples with saw-cut surfaces showed a large reduction in surface roughness after 7 days of reaction in either solution. Reaction in silicate solution for up to 91 days produced no further change in surface morphology, while reaction in DIW produced a spongy surface that formed the substrate for further surface layer development. The differences in the surface morphology of the samples may create microclimates that control the details of development of alteration layers on the glass; however, the concentrations of elements in leaching solutions show differences of 50% or less between samples prepared with different surface conditions for tests of a few months duration. 6 refs., 7 figs., 1 tab.
- Report Numbers
- E 1.99:ucrl-jc-103653
E 1.99: conf-9011116--6
conf-9011116--6
ucrl-jc-103653 - Subject(s)
- Other Subject(s)
- Glass
- Surface Properties
- Aqueous Solutions
- Compiled Data
- Leachates
- Leaching
- Microstructure
- Performance
- Sample Preparation
- Silicates
- Vitrification
- Waste Processing
- Water
- Crystal Structure
- Data
- Dispersions
- Dissolution
- Hydrogen Compounds
- Information
- Management
- Mixtures
- Numerical Data
- Oxygen Compounds
- Processing
- Separation Processes
- Silicon Compounds
- Solutions
- Waste Management
- Note
- Published through SciTech Connect.
10/24/1990.
"ucrl-jc-103653"
" conf-9011116--6"
"DE91005263"
14. nuclear waste management conference, Boston, MA (USA), 26-29 Nov 1990.
Oversby, V.M.; Oh, M.S. - Funding Information
- W-7405-ENG-48
View MARC record | catkey: 14417880