Washington, D.C. : United States. Dept. of Energy, 2009. Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy.
We report the results of single-crystal neutron diffraction studies of the superconductor BaNi₂As₂. The experiments were performed on a tiny crystal of mass 0.8 mg at several temperatures between 20 and 200 K using the Single Crystal Diffractometer, SCD, at the Los Alamos Neutron Science Center. Above 130 K, BaNi₂As₂ crystallizes in the tetragonal ThCr₂Si₂ structure. Our neutron diffraction data corroborate a first-order structural transition around 130 K with a relatively large hysteresis of about 10K, in agreement with observations from bulk studies. The anisotropic thermal displacement coefficients are enhanced along c-axis approaching the transition, and a splitting is observed for in-plane type reflections below the transition, which is evidence for a change in crystal structure.
Report Numbers
E 1.99:la-ur-09-03692 E 1.99: la-ur-09-3692 la-ur-09-3692 la-ur-09-03692
Published through SciTech Connect. 01/01/2009. "la-ur-09-03692" " la-ur-09-3692" FT Nakotte, Heinz; Kothapalli, Karunakar; Ronning, F; Bauer, E D; Schultz, A J.