Synthesis of picryl chloride [electronic resource].
- Published:
- Washington, D.C. : United States. Dept. of Energy, 1970.
Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy. - Physical Description:
- 22 pages : digital, PDF file
- Additional Creators:
- United States. Department of Energy and United States. Department of Energy. Office of Scientific and Technical Information
Access Online
- Restrictions on Access:
- Free-to-read Unrestricted online access
- Summary:
- A total of six pilot-scale batches of picryl chloride were made. These included three 5-kg batches and three 10-kg batches. The three 5-kg batches were made to investigate the problems encountered with actual production and materials handling. The three 10-kg batches were made to study the process parameters and the yield problems originally encountered with the 5-kg batches. The yields on the 5-kg batches ranged from 40 to 60% of approximately 50% purity. The yields on the 10-kg batches were 80, 86 and 91% in chronological order. The purities were 95, 99+ and 99+% respectively.
- Report Numbers:
- E 1.99:mhsmp--70-16
mhsmp--70-16 - Subject(s):
- Other Subject(s):
- Note:
- Published through SciTech Connect.
07/01/1970.
"mhsmp--70-16"
"DE97008918"
Hayes, D.V.; Honea, F.I.
Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (United States) - Funding Information:
- AC04-91AL65030
View MARC record | catkey: 14657344