Method to Determine Oxalate in High-Level Sludge by Ion Chromatography [electronic resource].
Published
Washington, D.C. : United States. Dept. of Energy, 2002. Oak Ridge, Tenn. : Distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy.
The Sludge Batch 3 macrobatch feed to the DWPF is expected to contain a relatively high concentration of oxalate. A simple acid addition at room temperature has been shown to be in high-level sludge. This sample preparation requires only about five minutes and yields solutions suitable for oxalate determinations by ion chromatography.