The development of experimental setups and procedures is considered for calibrating photosensitive devices in the spectral range 1022 to 2500 A for which no direct calibration techniques exist. An indirect technique that uses a sodium salicylate detector calibrated outside this range was developed for use as a secondary standard. The primary standard was a xenon-filled ionization chamber, which is an absolute standard over the wavelength interval 972 to 1022 A. Measurements made by this method were checked at 1470 A with a xenon lamp and at 2537 A with a mercury arc lamp and a 0.5 m blaze monochromator with a grating blazed at 2000 A. The overall accuracy of the measurements was + or - 40 percent or better.