Procedures used to standardize the strengths of a number of encapsulated gamma sources used to calibrate the sensitivity of Compton and pair scintillation gamma spectrometers designed to determine the spectrum of prompt gamma rays from fission of U/sup 2//sup 3//sup 5/ are described. Calibration of the ion-chamber response vs. source intensity was accomplished using calibration data obtained by W. S. Lyon. Instrumental drifts as a function of time were compensated using the observed response to long-lived sources. Calibration of the absolute efficiency of the chamber for various radioactive isotopes was performed in a method, based on an approximate calculation of this efficiency from crosssection data, on a number of absolute source calibrations using coincidence techniques, and on the existing ionchamber efficiency ratios determined by W. S. Lyon. Attention was given to detailed estimates of the accuracy of the procedures used. (auth)