A method is presented for the determination of uranium (as U/sup 238/) in uraniuni-loaded graphite fuel elenients by a non-destructive, direct radioactivity analysis technique. A 200-cbannel pulse-height analyzer, equipped with a 3 in. x 3 in. NaI(Tl) crystal, is used to measure the Np/sup 239/ radioactivity of the neutron-irradiated samples. The amount of U/sup 238/ in the test samples is deterimined quantitatively by comparing the Np/sup 239/ radioactivity induced in each sample with the Np/sup 239/ radioactivity induced into known standards of U/sup 238/ processed under the same conditions as the test samples. The limit of detection for U/sup 238/in samples of normal uranium composition for this method is about 1.0 x l0-4 ug. (auth)
U.S. Atomic Energy Commission depository collection.
Note
DOE contract number: W-7405-ENG-26 NSA number: NSA-16-004135 OSTI Identifier 4828291 Research organization: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States).