Mass spectrometric analytical services and research activities to support coal-liquid characterization research. Quarterly report, June 9, 1976--October 5, 1976. [10 refs].
- Author
- Scheppele, S. E.
- Published
- United States : [publisher not identified], 1976.
[Oak Ridge, Tennessee] : [U.S. Atomic Energy Commission], 1976. - Physical Description
- microfiche : negative ; 11 x 15 cm
- Summary
- Low-resolution field ionization and high-resolution 70-eV electron-impact mass spectra data were obtained for 28 GPC fractions acquired from Bartlett, Kansas, heavy petroleum by members of the Separation and Characterization group at the Bartlesville Energy Research Center. This group was supplied with most-probable empirical formulas deduced from the high resolution electron-impact data. Analysis of the qualitative and quantitative analytical data previously obtained for GPC fractions from a Synthoil sample by high- and low-resolution field-ionization and high-resolution 70-eV electron-impact mass spectrometry is essentially complete. A study of field-ionization sensitivities for saturates and mixtures of saturates and aromatics is in progress. Components required to modify the combined FI/EI ion source to permit operation in the field desorption mode have been ordered.
- Report Numbers
- COO-0020-5
- Other Subject(s)
- 01 coal, lignite, and peat
- 010600 - coal, lignite, & peat- properties & composition
- 02 petroleum
- 023000 - petroleum- properties & composition
- Chemical analysis
- Coal liquefaction
- Coal liquids
- Energy sources
- Fossil fuels
- Fuels
- Liquefaction
- Mass spectra
- Petroleum
- Qualitative chemical analysis
- Quantitative chemical analysis
- Spectra
- Synthoil process
- Collection
- U.S. Atomic Energy Commission depository collection.
- Note
- DOE contract number: EY-76-S-02-0020
OSTI Identifier 7238026
Research organization: Oklahoma State Univ., Stillwater (USA). Dept. of Chemistry.
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