Liquid chromatographic analysis of nitration of diphenylamine stabilizer in explosives. [PBX-9404].

Author: MacDougall, C. S.
Published: United States : [publisher not identified], 1975.
[Oak Ridge, Tennessee] : [U.S. Atomic Energy Commission], 1975.
Physical Description: microfiche : negative ; 11 x 15 cm

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Summary

A high speed liquid chromatographic method was developed for the quantitative analysis of nitrated diphenylamines in PBX-9404. The procedure included extraction of the nitrated diphenylamines into methylene chloride, followed by chromatographic separation and examination of the various species. The method requires a 10-g sample of high explosive in order to provide a sample of nitro DPA suitably concentrated for chromatographic analysis. (auth)

Report Numbers

MHSMP-75-58

Other Subject(s)

Collection

U.S. Atomic Energy Commission depository collection.

Note

OSTI Identifier 7199723
Research organization: Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (United States).

View MARC record | catkey: 45895195